Glass-ceramic matrix composites : liquid molding and mechanical behavior

This research work is part of the collaborative project COMPTINN (Innovative composite materials for intermediate temperature applications). This project aims at enabling the manufacturing of competitive structural composites able to bear up continuous thermal exposure, such as in aircraft parts located close to engines. A new class of glass-ceramic matrices for structural composites was developed to reach this goal. These new matrices come from an inorganic thermosetting polymer derived from a geopolymeric system. Prepreg process is currently used to manufacture composites but these composites would be more competitive if they are produced by an easy and cost effective process technology. Liquid molding (LRI or RTM) seems to be a convenient solution. Two kinds of reinforcements were considered: a layup of several two-dimensional woven fabric plies and a three-dimensional preform.The rheological behaviour of the considered inorganic polymer was firstly investigated. The best conditions were identified to obtain the lowest viscosity of the resin in order to help the production of structural composite parts by liquid molding.Then, the research work investigates how changes in the manufacturing process impact the mechanical properties of the composites. A microstructural characterization helps to link the mechanical behavior to the processing route. The effects of varying several processing parameters have been studied such as the dilution rate of the resin, the impregnation direction or the pressure differential.

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Source https://theses.hal.science/tel-00977974
Author Farrugia, Anaïs
Maintainer CCSD
Last Updated May 5, 2026, 15:02 (UTC)
Created May 5, 2026, 15:02 (UTC)
Identifier NNT: 2013EMAC0002
Language fr
Rights https://about.hal.science/hal-authorisation-v1/
contributor Institut Clément Ader (ICA) ; Institut Supérieur de l'Aéronautique et de l'Espace (ISAE-SUPAERO)-Institut National des Sciences Appliquées - Toulouse (INSA Toulouse) ; Institut National des Sciences Appliquées (INSA)-Communauté d'universités et établissements de Toulouse (Comue de Toulouse)-Institut National des Sciences Appliquées (INSA)-Communauté d'universités et établissements de Toulouse (Comue de Toulouse)-Université Toulouse III - Paul Sabatier (UT3) ; Communauté d'universités et établissements de Toulouse (Comue de Toulouse)-Centre National de la Recherche Scientifique (CNRS)-IMT École nationale supérieure des Mines d'Albi-Carmaux (IMT Mines Albi) ; Institut Mines-Télécom [Paris] (IMT)-Communauté d'universités et établissements de Toulouse (Comue de Toulouse)-Institut Mines-Télécom [Paris] (IMT)
creator Farrugia, Anaïs
date 2013-12-09T00:00:00
harvest_object_id fdb859c0-97f2-4dc7-8922-d730919207bd
harvest_source_id 3374d638-d20b-4672-ba96-a23232d55657
harvest_source_title test moissonnage SELUNE
metadata_modified 2026-03-31T00:00:00
set_spec type:THESE