Synthesis of tubular SiC thick CVD coatings for thermostructural applications

The goal of this study was to synthesize monolithic SiC tubes to improve sealing of the SiC / SiC composite of a nuclear fuel cladding structure. Tubes of 8 mm inner diameter and several hundred micrometers in thickness have been produced by atmospheric pressure chemical vapor deposition (APCVD) from a mixture CH3SiHCl2/H2. The method has been developed so as to produce continuous SiC tubes of up to thirty centimeters long. The chemical composition and microstructure of the tubes were determined by microprobe, Raman spectroscopy, XRD and electron microscopy (SEM, TEM). The mechanical properties of the tubes were characterized by nanoindentation tests and through compression C -ring . The thermomechanical behavior was also studied. The method includes consideration of a thermokinetic study , followed by a gas phase analysis by IRTF and 2D modeling of the reactor.

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Source https://theses.hal.science/tel-00958465
Author Drieux, Patxi
Maintainer CCSD
Last Updated May 6, 2026, 01:44 (UTC)
Created May 6, 2026, 01:44 (UTC)
Identifier NNT: 2013BOR15203
Language fr
Rights https://about.hal.science/hal-authorisation-v1/
contributor Laboratoire des Composites Thermostructuraux (LCTS) ; Université de Bordeaux (UB)-Commissariat à l'énergie atomique et aux énergies alternatives (CEA)-SAFRAN Group-Institut de Chimie - CNRS Chimie (INC-CNRS)-Centre National de la Recherche Scientifique (CNRS)
creator Drieux, Patxi
date 2013-12-19T00:00:00
harvest_object_id fbcb5f35-4586-4ae0-b2aa-d14534900166
harvest_source_id 3374d638-d20b-4672-ba96-a23232d55657
harvest_source_title test moissonnage SELUNE
metadata_modified 2026-03-31T00:00:00
set_spec type:THESE