in situ Microtomography applied to deformation and solidification of aluminium alloys

Hot tearing is a defect which forms at high solid fraction in solidifying alloys, when the material is still semi solid. This work aims at bringing a contribution to the prevision of this phenomenon. To be able to do that, it is necessary to characterize deformability of the semi-solid alloy solid phase, and also bring local information on microstructure during its straining (liquid and pore fractions, liquid films thickness, liquid flow velocity…). Solid phase macroscopic behaviour on solidus line has been determined and validated by hot compression tests. The calculated behaviour law has also been compared with several analytical models. Mechanical behaviour differences between homogeneous and composition gradient microstructure has been put in evidence. Real time microscopic information on tensile tested semi solid samples have been obtained by in situ standard microtomography, in isothermal and solidification conditions. An analytic hot tearing predictive model has been modified to better fit the experimental data. An experimental device has been developed and realized to be able to carry out high and ultra high speed microtomography. These two methods bring better both time and space resolution. High velocity phenomenons in very fine microstructures can thus be visible. Isothermal and solidification conditions tests and now reproducible on remelted samples.

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Source https://theses.hal.science/tel-00919754
Author Mireux, Bastien
Maintainer CCSD
Last Updated May 7, 2026, 18:49 (UTC)
Created May 7, 2026, 18:49 (UTC)
Identifier NNT: 2012GRENI081
Language fr
Rights https://about.hal.science/hal-authorisation-v1/
contributor Science et Ingénierie des Matériaux et Procédés (SIMaP) ; Université Joseph Fourier - Grenoble 1 (UJF)-Institut polytechnique de Grenoble - Grenoble Institute of Technology (Grenoble INP)-Institut National Polytechnique de Grenoble (INPG)-Institut de Chimie - CNRS Chimie (INC-CNRS)-Centre National de la Recherche Scientifique (CNRS)
creator Mireux, Bastien
date 2012-11-13T00:00:00
harvest_object_id a5d5ef94-51c0-4454-843a-5598971fbb20
harvest_source_id 3374d638-d20b-4672-ba96-a23232d55657
harvest_source_title test moissonnage SELUNE
metadata_modified 2026-03-31T00:00:00
set_spec type:THESE