SEARCH FOR MORPHOLOGICAL PARAMETERS INFLUENTIAL FOR PREDICTION OF THE MECHANICAL CHARACTERISTICS OF AN AUSTENOFERRITIC DUPLEX STAINLESS STEEL

Duplex stainless steels are commonly used ( among others in nuclear industry) for their good properties. However these steels may "age" in service condition at high temperatures. As their mechanical properties ( charpy impact toughness, resistance to ductile tearing) are often very scattered and tend to decrease after ageing, it has become essential to predict them with high precision. For this, we propose to explain a part of the scattering of the mechanical properties with measurable parameters in relation with the particularly complicated two-phase morphology. The two-phase and bipercolated morphology of the ferrite and austenite phases is first characterised from the observation of 2D images and from the reconstitution of a 3D image. At the same time we precise the genesis of the formation's mechanisms of the structure (germination and growth of the austenitic phase in the solidified ferri tic one) in relation with the literature. The morphological characteristics so observed corresponding with classical notions of mathematical morphology, -size, covariance, connexity-, we use morphological operators to measure morphological variables by image analysis. We establish then a link between toughness and a parameter measuring fineness of the morphology. The lack of data for very aged steels prevent us from proposing a model of toughness which could take this parameter into consideration at these ageing states, for which it is properly the more crucial to obtain specially precise predictions. _A mathematical mo del of the 3D structure of the steel is finally proposed. We choose an homogeneous Markov chain of 3D spatial processes, whose evolution in time mimes the solidification. The morphology of the microstructure is so summarised with 8 parameters. This model is liable to be coupled with a model of toughness, for which it would so enlarge the possibilities of prediction. It could also be used to simulate subsequently the damage and the rupture of two-phase materials.

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Source https://theses.hal.science/tel-00817970
Author Messiaen, Laure
Maintainer CCSD
Last Updated May 11, 2026, 07:08 (UTC)
Created May 11, 2026, 07:08 (UTC)
Identifier NNT: 1997ENMP0764
Language fr
Rights https://about.hal.science/hal-authorisation-v1/
contributor Département Informatique - ENSMSE ; École des Mines de Saint-Étienne (Mines Saint-Étienne MSE) ; Institut Mines-Télécom [Paris] (IMT)-Institut Mines-Télécom [Paris] (IMT)
creator Messiaen, Laure
date 1997-06-17T00:00:00
harvest_object_id b556dbc0-fcc7-4cb0-babc-92000621e0eb
harvest_source_id 3374d638-d20b-4672-ba96-a23232d55657
harvest_source_title test moissonnage SELUNE
metadata_modified 2026-01-19T00:00:00
set_spec type:THESE